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Beilstein J. Org. Chem. 2010, 6, 1206–1210, doi:10.3762/bjoc.6.138
Graphical Abstract
Scheme 1: Retrosynthetic analysis outlining the stereocontrolled construction of the aminopolyol core of (−)-...
Scheme 2: Depictions of the likely major conformations of the siloxane (A) and disiloxane (B) rings.
Scheme 3: Confirmation of the relative stereochemistry of bis(triazoline) 14a. (a) TfOH, CH3CN, rt, 18 h; (b)...